By Marvin J. Weinstein and Gerald H. Wagman (Eds.)
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Additional resources for ANTIBIOTICS: ISOLATION, SEPARATION AND PURIFICATION
J a i n , T. D . S a k o r e and C. E. Nordman, N a t u r e N e w B i o l . 231 (1971) 200-205. 98. S. C. J a i n and H . M . S o b e l l , J . Mol. B i o l . 6 8 (1972) 1-20. 39 Ansamycins . A K Ganguly Chemical Research Department Schering Corporation. Bloomfield. J. 2. 1 Ansamycins: General introduction ................. 3 Structure.. 4 Structure 2 . 1 1 Rifamycin Y ................................ ......................... ................................. ....................... .................................
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Ticub Hydroxyproline and altohydroxyproline, from actinomycins X o a and X o B , respectively, were distinguished by HVE16’28. This separation can also be effected by GLC72. The latter technique was employed to distinguish c i b - and thanb-4-methylproline in the actinomycins Klc, KzC and Kit, KZt, respectively+ The two diastereoisomers of 4 - h y d r o x y - 5 - m e t h y l p r o l i n e resulting from aluminum isopropoxide reduction of 4-keto-5methylproline in intact actinomycins Z 1 and 25 were distinguished b high-voltage paper electrophoresis, but were not identified 5zy73.
ANTIBIOTICS: ISOLATION, SEPARATION AND PURIFICATION by Marvin J. Weinstein and Gerald H. Wagman (Eds.)